A reaction cell for in situ studies of hydrothermal titration

P. Norby; C. Cahill; C. Koleda; J. B. Parise

doi:10.1107/S002188989701337X

A reaction cell for in situ studies of hydrothermal titration

P. Norby
, C. Cahill
, C. Koleda
, J. B. Parise

Geosciences

Stony Brook University

Research output: Contribution to journal › Article › peer-review

24 Scopus citations

Abstract

A reaction cell for in situ studies of both ion-exchange and hydrothermal titration reactions has been designed and built. This cell allows the injection of reagents into a reaction mixture over time during X-ray data collection. A demonstration experiment followed the injection of Na₂SO₄(aq) into BaCl₂(aq) to yield a time-resolved X-ray powder diffraction pattern of the precipitation of BaSO₄(s).

Original language	English
Pages (from-to)	481-483
Number of pages	3
Journal	Journal of Applied Crystallography
Volume	31
Issue number	3
DOIs	https://doi.org/10.1107/S002188989701337X
State	Published - Jun 1 1998

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title = "A reaction cell for in situ studies of hydrothermal titration",

abstract = "A reaction cell for in situ studies of both ion-exchange and hydrothermal titration reactions has been designed and built. This cell allows the injection of reagents into a reaction mixture over time during X-ray data collection. A demonstration experiment followed the injection of Na2SO4(aq) into BaCl2(aq) to yield a time-resolved X-ray powder diffraction pattern of the precipitation of BaSO4(s).",

author = "P. Norby and C. Cahill and C. Koleda and Parise, \{J. B.\}",

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T1 - A reaction cell for in situ studies of hydrothermal titration

AU - Norby, P.

AU - Cahill, C.

AU - Koleda, C.

AU - Parise, J. B.

PY - 1998/6/1

Y1 - 1998/6/1

N2 - A reaction cell for in situ studies of both ion-exchange and hydrothermal titration reactions has been designed and built. This cell allows the injection of reagents into a reaction mixture over time during X-ray data collection. A demonstration experiment followed the injection of Na2SO4(aq) into BaCl2(aq) to yield a time-resolved X-ray powder diffraction pattern of the precipitation of BaSO4(s).

AB - A reaction cell for in situ studies of both ion-exchange and hydrothermal titration reactions has been designed and built. This cell allows the injection of reagents into a reaction mixture over time during X-ray data collection. A demonstration experiment followed the injection of Na2SO4(aq) into BaCl2(aq) to yield a time-resolved X-ray powder diffraction pattern of the precipitation of BaSO4(s).

UR - https://www.scopus.com/pages/publications/0006944789

U2 - 10.1107/S002188989701337X

DO - 10.1107/S002188989701337X

M3 - Article

AN - SCOPUS:0006944789

SN - 0021-8898

VL - 31

SP - 481

EP - 483

JO - Journal of Applied Crystallography

JF - Journal of Applied Crystallography

IS - 3

ER -

A reaction cell for in situ studies of hydrothermal titration

Abstract

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