A versatile sample-environment cell for non-ambient X-ray scattering experiments

Peter J. Chupas; Karena W. Chapman; Charles Kurtz; Jonathan C. Hanson; Peter L. Lee; Clare P. Grey

doi:10.1107/S0021889808020165

A versatile sample-environment cell for non-ambient X-ray scattering experiments

Peter J. Chupas
, Karena W. Chapman
, Charles Kurtz
, Jonathan C. Hanson
, Peter L. Lee
, Clare P. Grey

Chemistry

Argonne National Laboratory
Brookhaven National Laboratory
Stony Brook University

Research output: Contribution to journal › Article › peer-review

296 Scopus citations

Abstract

A compact reaction cell is described for in-situ experiments requiring control of both the temperature of the sample and the atmosphere over the sample. The cell incorporates an optional furnace capable of temperatures of up to ∼1273 K. The compact design and ability of the cell to mount directly on a standard goniometer head allows portability to a large number of diffraction instruments at synchrotron sources.

Original language	English
Pages (from-to)	822-824
Number of pages	3
Journal	Journal of Applied Crystallography
Volume	41
Issue number	4
DOIs	https://doi.org/10.1107/S0021889808020165
State	Published - 2008

Keywords

Flow-cells
Furnaces
In-situ diffraction
Non-ambient conditions
X-ray scattering

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10.1107/S0021889808020165

Cite this

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title = "A versatile sample-environment cell for non-ambient X-ray scattering experiments",

abstract = "A compact reaction cell is described for in-situ experiments requiring control of both the temperature of the sample and the atmosphere over the sample. The cell incorporates an optional furnace capable of temperatures of up to ∼1273 K. The compact design and ability of the cell to mount directly on a standard goniometer head allows portability to a large number of diffraction instruments at synchrotron sources.",

keywords = "Flow-cells, Furnaces, In-situ diffraction, Non-ambient conditions, X-ray scattering",

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AU - Chupas, Peter J.

AU - Chapman, Karena W.

AU - Kurtz, Charles

AU - Hanson, Jonathan C.

AU - Lee, Peter L.

AU - Grey, Clare P.

PY - 2008

Y1 - 2008

N2 - A compact reaction cell is described for in-situ experiments requiring control of both the temperature of the sample and the atmosphere over the sample. The cell incorporates an optional furnace capable of temperatures of up to ∼1273 K. The compact design and ability of the cell to mount directly on a standard goniometer head allows portability to a large number of diffraction instruments at synchrotron sources.

AB - A compact reaction cell is described for in-situ experiments requiring control of both the temperature of the sample and the atmosphere over the sample. The cell incorporates an optional furnace capable of temperatures of up to ∼1273 K. The compact design and ability of the cell to mount directly on a standard goniometer head allows portability to a large number of diffraction instruments at synchrotron sources.

KW - Flow-cells

KW - Furnaces

KW - In-situ diffraction

KW - Non-ambient conditions

KW - X-ray scattering

UR - https://www.scopus.com/pages/publications/47549086507

U2 - 10.1107/S0021889808020165

DO - 10.1107/S0021889808020165

M3 - Article

AN - SCOPUS:47549086507

SN - 0021-8898

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JO - Journal of Applied Crystallography

JF - Journal of Applied Crystallography

IS - 4

ER -

A versatile sample-environment cell for non-ambient X-ray scattering experiments

Abstract

Keywords

Access to Document

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