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Development of in situ full field spectroscopic imaging analysis and application on li-ion battery using transmission x-ray microscopy

  • Brookhaven National Laboratory

Research output: Chapter in Book/Report/Conference proceedingConference contributionpeer-review

3 Scopus citations

Abstract

This paper presents the advance in spectroscopic imaging technique and analysis method from the newly developed transmission x-ray microscopy (TXM) at the beamline X8C of National Synchrotron Light Source. Through leastsquares linear combination fitting we developed on the in situ spectroscopic images, a time-dependent and spatially resolved chemical composition mapping can be obtained and quantitatively analyzed undergone chemical/electrochemical reactions. A correlation of morphological evolution, chemical state distribution changes and reaction conditions can be revealed. We successfully applied this method to study the electrochemical evolution of CuO, an anode material of Li-ion battery, during the lithiation-delitiation cycling.

Original languageEnglish
Title of host publicationX-Ray Nanoimaging
Subtitle of host publicationInstruments and Methods
PublisherSPIE
ISBN (Print)9780819497017
DOIs
StatePublished - 2013
EventX-Ray Nanoimaging: Instruments and Methods - San Diego, CA, United States
Duration: Aug 28 2013Aug 29 2013

Publication series

NameProceedings of SPIE - The International Society for Optical Engineering
Volume8851
ISSN (Print)0277-786X
ISSN (Electronic)1996-756X

Conference

ConferenceX-Ray Nanoimaging: Instruments and Methods
Country/TerritoryUnited States
CitySan Diego, CA
Period08/28/1308/29/13

Keywords

  • Battery
  • Spectroscopic Imaging
  • Transmission X-ray Microscopy
  • TXM
  • XANES imaging

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