Electrospun tungsten oxide nanofibers: Fabrication and characterization

Guan Wang; Xianrong Huang; Xiaoqing Yang; Pelagia Irene Gouma; Michael Dudley

doi:10.1557/proc-0915-r06-15

Electrospun tungsten oxide nanofibers: Fabrication and characterization

Guan Wang
, Xianrong Huang
, Xiaoqing Yang
, Pelagia Irene Gouma
, Michael Dudley

Materials Science and Engineering

Stony Brook University
Brookhaven National Laboratory

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

Abstract

Tungsten oxide nanofibers have been successfully fabricated in a way based on electrospinning technique. A DMF solution of Poly(Vinyl Acetate)(PVAc, Mw=500,000) was mixed with tungsten isopropoxide to form a viscous precursor solution. Composite nanofibers were obtained by electrspinning this viscous solution. By calcination of the composite fibers, pure tungsten oxide nanofibers were obtained with controllable diameters of around 100 nm. Morphology of the fibers has been characterized by SEM and TEM. The relationship between solution concentration and ceramic nanofiber morphology has been studied. The detailed structure evolution process has been investigated by synchrotron based in-situ XRD. Specific phases of the oxide nanofibers at various calcination temperatures have been obtained from the in-situ XRD spectrum.

Original language	English
Title of host publication	Nanostructured Materials and Hybrid Composites for Gas Sensors and Biomedical Applications
Publisher	Materials Research Society
Pages	155-160
Number of pages	6
ISBN (Print)	9781558998711
DOIs	https://doi.org/10.1557/proc-0915-r06-15
State	Published - 2006
Event	2006 Materials Research Society Spring Meeting - San Francisco, CA, United States Duration: Apr 18 2006 → Apr 20 2006

Publication series

Name	Materials Research Society Symposium Proceedings
Volume	915
ISSN (Print)	0272-9172

Conference

Conference	2006 Materials Research Society Spring Meeting
Country/Territory	United States
City	San Francisco, CA
Period	04/18/06 → 04/20/06

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10.1557/proc-0915-r06-15

Cite this

Wang, G., Huang, X., Yang, X., Gouma, P. I., & Dudley, M. (2006). Electrospun tungsten oxide nanofibers: Fabrication and characterization. In Nanostructured Materials and Hybrid Composites for Gas Sensors and Biomedical Applications (pp. 155-160). (Materials Research Society Symposium Proceedings; Vol. 915). Materials Research Society. https://doi.org/10.1557/proc-0915-r06-15

@inproceedings{e44934395cf84a1eaac9f8af27fcf6bb,

title = "Electrospun tungsten oxide nanofibers: Fabrication and characterization",

abstract = "Tungsten oxide nanofibers have been successfully fabricated in a way based on electrospinning technique. A DMF solution of Poly(Vinyl Acetate)(PVAc, Mw=500,000) was mixed with tungsten isopropoxide to form a viscous precursor solution. Composite nanofibers were obtained by electrspinning this viscous solution. By calcination of the composite fibers, pure tungsten oxide nanofibers were obtained with controllable diameters of around 100 nm. Morphology of the fibers has been characterized by SEM and TEM. The relationship between solution concentration and ceramic nanofiber morphology has been studied. The detailed structure evolution process has been investigated by synchrotron based in-situ XRD. Specific phases of the oxide nanofibers at various calcination temperatures have been obtained from the in-situ XRD spectrum.",

author = "Guan Wang and Xianrong Huang and Xiaoqing Yang and Gouma, \{Pelagia Irene\} and Michael Dudley",

year = "2006",

doi = "10.1557/proc-0915-r06-15",

language = "English",

isbn = "9781558998711",

series = "Materials Research Society Symposium Proceedings",

publisher = "Materials Research Society",

pages = "155--160",

booktitle = "Nanostructured Materials and Hybrid Composites for Gas Sensors and Biomedical Applications",

note = "2006 Materials Research Society Spring Meeting ; Conference date: 18-04-2006 Through 20-04-2006",

}

Wang, G, Huang, X, Yang, X, Gouma, PI & Dudley, M 2006, Electrospun tungsten oxide nanofibers: Fabrication and characterization. in Nanostructured Materials and Hybrid Composites for Gas Sensors and Biomedical Applications. Materials Research Society Symposium Proceedings, vol. 915, Materials Research Society, pp. 155-160, 2006 Materials Research Society Spring Meeting, San Francisco, CA, United States, 04/18/06. https://doi.org/10.1557/proc-0915-r06-15

Electrospun tungsten oxide nanofibers: Fabrication and characterization. / Wang, Guan; Huang, Xianrong; Yang, Xiaoqing et al.
Nanostructured Materials and Hybrid Composites for Gas Sensors and Biomedical Applications. Materials Research Society, 2006. p. 155-160 (Materials Research Society Symposium Proceedings; Vol. 915).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

TY - GEN

T1 - Electrospun tungsten oxide nanofibers

T2 - 2006 Materials Research Society Spring Meeting

AU - Wang, Guan

AU - Huang, Xianrong

AU - Yang, Xiaoqing

AU - Gouma, Pelagia Irene

AU - Dudley, Michael

PY - 2006

Y1 - 2006

N2 - Tungsten oxide nanofibers have been successfully fabricated in a way based on electrospinning technique. A DMF solution of Poly(Vinyl Acetate)(PVAc, Mw=500,000) was mixed with tungsten isopropoxide to form a viscous precursor solution. Composite nanofibers were obtained by electrspinning this viscous solution. By calcination of the composite fibers, pure tungsten oxide nanofibers were obtained with controllable diameters of around 100 nm. Morphology of the fibers has been characterized by SEM and TEM. The relationship between solution concentration and ceramic nanofiber morphology has been studied. The detailed structure evolution process has been investigated by synchrotron based in-situ XRD. Specific phases of the oxide nanofibers at various calcination temperatures have been obtained from the in-situ XRD spectrum.

AB - Tungsten oxide nanofibers have been successfully fabricated in a way based on electrospinning technique. A DMF solution of Poly(Vinyl Acetate)(PVAc, Mw=500,000) was mixed with tungsten isopropoxide to form a viscous precursor solution. Composite nanofibers were obtained by electrspinning this viscous solution. By calcination of the composite fibers, pure tungsten oxide nanofibers were obtained with controllable diameters of around 100 nm. Morphology of the fibers has been characterized by SEM and TEM. The relationship between solution concentration and ceramic nanofiber morphology has been studied. The detailed structure evolution process has been investigated by synchrotron based in-situ XRD. Specific phases of the oxide nanofibers at various calcination temperatures have been obtained from the in-situ XRD spectrum.

UR - https://www.scopus.com/pages/publications/33749367015

U2 - 10.1557/proc-0915-r06-15

DO - 10.1557/proc-0915-r06-15

M3 - Conference contribution

AN - SCOPUS:33749367015

SN - 9781558998711

T3 - Materials Research Society Symposium Proceedings

SP - 155

EP - 160

BT - Nanostructured Materials and Hybrid Composites for Gas Sensors and Biomedical Applications

PB - Materials Research Society

Y2 - 18 April 2006 through 20 April 2006

ER -

Electrospun tungsten oxide nanofibers: Fabrication and characterization

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