Hydrostatic low-range pressure applications of the Paris-Edinburgh cell utilizing polymer gaskets for diffuse X-ray scattering measurements

Karena W. Chapman; Peter J. Chupas; Charles A. Kurtz; Darren R. Locke; John B. Parise; Joseph A. Hriljac

doi:10.1107/S0021889806047923

Hydrostatic low-range pressure applications of the Paris-Edinburgh cell utilizing polymer gaskets for diffuse X-ray scattering measurements

Karena W. Chapman
, Peter J. Chupas
, Charles A. Kurtz
, Darren R. Locke
, John B. Parise
, Joseph A. Hriljac

United States Department of Energy
Stony Brook University
University of Birmingham

Research output: Contribution to journal › Article › peer-review

13 Scopus citations

Abstract

The use of a polymeric Torlon (polyamide-imide) gasket material in a Paris-Edinburgh pressure cell for in situ high-pressure X-ray scattering measurements is demonstrated. The relatively low bulk modulus of the gasket allows for fine control of the sample pressure over the range 0.01-0.42 GPa. The quality of the data obtained in this way is suitable for Bragg and pair distribution function analysis.

Original language	English
Article number	he5355
Pages (from-to)	196-198
Number of pages	3
Journal	Journal of Applied Crystallography
Volume	40
Issue number	1
DOIs	https://doi.org/10.1107/S0021889806047923
State	Published - Jan 12 2007

Keywords

Diffuse scattering
High pressure
Pair distribution function
Paris-Edinburgh cell

Access to Document

10.1107/S0021889806047923

Cite this

@article{368e80204d6c46ffa17178aabc61efaa,

title = "Hydrostatic low-range pressure applications of the Paris-Edinburgh cell utilizing polymer gaskets for diffuse X-ray scattering measurements",

abstract = "The use of a polymeric Torlon (polyamide-imide) gasket material in a Paris-Edinburgh pressure cell for in situ high-pressure X-ray scattering measurements is demonstrated. The relatively low bulk modulus of the gasket allows for fine control of the sample pressure over the range 0.01-0.42 GPa. The quality of the data obtained in this way is suitable for Bragg and pair distribution function analysis.",

keywords = "Diffuse scattering, High pressure, Pair distribution function, Paris-Edinburgh cell",

author = "Chapman, \{Karena W.\} and Chupas, \{Peter J.\} and Kurtz, \{Charles A.\} and Locke, \{Darren R.\} and Parise, \{John B.\} and Hriljac, \{Joseph A.\}",

year = "2007",

month = jan,

day = "12",

doi = "10.1107/S0021889806047923",

language = "English",

volume = "40",

pages = "196--198",

journal = "Journal of Applied Crystallography",

issn = "0021-8898",

number = "1",

}

TY - JOUR

T1 - Hydrostatic low-range pressure applications of the Paris-Edinburgh cell utilizing polymer gaskets for diffuse X-ray scattering measurements

AU - Chapman, Karena W.

AU - Chupas, Peter J.

AU - Kurtz, Charles A.

AU - Locke, Darren R.

AU - Parise, John B.

AU - Hriljac, Joseph A.

PY - 2007/1/12

Y1 - 2007/1/12

N2 - The use of a polymeric Torlon (polyamide-imide) gasket material in a Paris-Edinburgh pressure cell for in situ high-pressure X-ray scattering measurements is demonstrated. The relatively low bulk modulus of the gasket allows for fine control of the sample pressure over the range 0.01-0.42 GPa. The quality of the data obtained in this way is suitable for Bragg and pair distribution function analysis.

AB - The use of a polymeric Torlon (polyamide-imide) gasket material in a Paris-Edinburgh pressure cell for in situ high-pressure X-ray scattering measurements is demonstrated. The relatively low bulk modulus of the gasket allows for fine control of the sample pressure over the range 0.01-0.42 GPa. The quality of the data obtained in this way is suitable for Bragg and pair distribution function analysis.

KW - Diffuse scattering

KW - High pressure

KW - Pair distribution function

KW - Paris-Edinburgh cell

UR - https://www.scopus.com/pages/publications/33846496772

U2 - 10.1107/S0021889806047923

DO - 10.1107/S0021889806047923

M3 - Article

AN - SCOPUS:33846496772

SN - 0021-8898

VL - 40

SP - 196

EP - 198

JO - Journal of Applied Crystallography

JF - Journal of Applied Crystallography

IS - 1

M1 - he5355

ER -

Hydrostatic low-range pressure applications of the Paris-Edinburgh cell utilizing polymer gaskets for diffuse X-ray scattering measurements

Abstract

Keywords

Access to Document

Other files and links

Fingerprint

Cite this