Abstract
The local environment of nickel in VSB-1, a nanoporous nickel phosphate material, was systematically investigated by a combination of X-ray absorption spectroscopy and multiple complementary techniques before and after calcination. A considerable unit cell shrinkage observed in VSB-1 after calcination is explained by the loss of F- ions and the corresponding changes in the nickel environment.
| Original language | English |
|---|---|
| Pages (from-to) | 157-162 |
| Number of pages | 6 |
| Journal | Microporous and Mesoporous Materials |
| Volume | 223 |
| DOIs | |
| State | Published - Mar 15 2016 |
Keywords
- Nickel phosphate
- TGA/DTG-DSC-MS
- UV-vis-NIR
- VSB-1
- XAFS
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