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Insight into the local environment of nickel in VSB-1 before and after calcination

  • Jianqiang Wang
  • , Zhendong Wang
  • , Zhenlong Jia
  • , Gen Meng
  • , Zhongqiang Xu
  • , Weimin Yang
  • , Anatoly I. Frenkel
  • SINOPEC

Research output: Contribution to journalArticlepeer-review

1 Scopus citations

Abstract

The local environment of nickel in VSB-1, a nanoporous nickel phosphate material, was systematically investigated by a combination of X-ray absorption spectroscopy and multiple complementary techniques before and after calcination. A considerable unit cell shrinkage observed in VSB-1 after calcination is explained by the loss of F- ions and the corresponding changes in the nickel environment.

Original languageEnglish
Pages (from-to)157-162
Number of pages6
JournalMicroporous and Mesoporous Materials
Volume223
DOIs
StatePublished - Mar 15 2016

Keywords

  • Nickel phosphate
  • TGA/DTG-DSC-MS
  • UV-vis-NIR
  • VSB-1
  • XAFS

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