Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)

H. P. Liermann; Z. Konopkova; K. Appel; C. Prescher; A. Schropp; V. Cerantola; R. J. Husband; J. D. McHardy; M. I. McMahon; R. S. McWilliams; C. M. Pepin; J. Mainberger; M. Roeper; A. Berghauser; H. Damker; P. Talkovski; M. Foese; N. Kujala; O. B. Ball; M. A. Baron; R. Briggs; M. Bykov; E. Bykova; J. Chantel; A. L. Coleman; H. Cynn; D. Dattelbaum; L. E. Dresselhaus-Marais; J. H. Eggert; L. Ehm; W. J. Evans; G. Fiquet; M. Frost; K. Glazyrin; A. F. Goncharov; H. Hwang; Zs Jenei; J. Y. Kim; F. Langenhorst; Y. Lee; M. Makita; H. Marquardt; E. E. McBride; S. Merkel; G. Morard; E. F. O'Bannon; C. Otzen; E. J. Pace; A. Pelka; J. S. Pigott; V. B. Prakapenka; R. Redmer; C. Sanchez-Valle; M. Schoelmerich; S. Speziale; G. Spiekermann; B. T. Sturtevant; S. Toleikis; N. Velisavljevic; M. Wilke; C. S. Yoo; C. Baehtz; U. Zastrau; C. Strohm

doi:10.1107/S1600577521002551

Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)

H. P. Liermann
, Z. Konopkova
, K. Appel
, C. Prescher
, A. Schropp
, V. Cerantola
, R. J. Husband
, J. D. McHardy
, M. I. McMahon
, R. S. McWilliams
, C. M. Pepin
, J. Mainberger
, M. Roeper
, A. Berghauser
, H. Damker
, P. Talkovski
, M. Foese
, N. Kujala
, O. B. Ball
, M. A. Baron

R. Briggs, M. Bykov, E. Bykova, J. Chantel, A. L. Coleman, H. Cynn, D. Dattelbaum, L. E. Dresselhaus-Marais, J. H. Eggert, L. Ehm, W. J. Evans, G. Fiquet, M. Frost, K. Glazyrin, A. F. Goncharov, H. Hwang, Zs Jenei, J. Y. Kim, F. Langenhorst, Y. Lee, M. Makita, H. Marquardt, E. E. McBride, S. Merkel, G. Morard, E. F. O'Bannon, C. Otzen, E. J. Pace, A. Pelka, J. S. Pigott, V. B. Prakapenka, R. Redmer, C. Sanchez-Valle, M. Schoelmerich, S. Speziale, G. Spiekermann, B. T. Sturtevant, S. Toleikis, N. Velisavljevic, M. Wilke, C. S. Yoo, C. Baehtz, U. Zastrau, C. Strohm

Geosciences

German Electron Synchrotron
European XFEL
University of Edinburgh
Commissariat à l’énergie atomique et aux énergies alternatives
Université Paris-SaclayCEA
Helmholtz-Zentrum Dresden-Rossendorf
Sorbonne Université
Lawrence Livermore National Laboratory
Carnegie Science
INRAE
Los Alamos National Laboratory
SLAC National Accelerator Laboratory
Yonsei University
Hanyang University
Friedrich Schiller University Jena
University of Oxford
Université de Grenoble Alpes, ISTerre
Case Western Reserve University
The University of Chicago
University of Rostock
University of Münster
Helmholtz Centre Potsdam - German Research Centre for Geosciences
University of Potsdam
Washington State University Pullman

Research output: Contribution to journal › Article › peer-review

32 Scopus citations

Abstract

The high-precision X-ray diffraction setup for work with diamond anvil cells (DACs) in interaction chamber 2 (IC2) of the High Energy Density instrument of the European X-ray Free-Electron Laser is described. This includes beamline optics, sample positioning and detector systems located in the multipurpose vacuum chamber. Concepts for pump-probe X-ray diffraction experiments in the DAC are described and their implementation demonstrated during the First User Community Assisted Commissioning experiment. X-ray heating and diffraction of Bi under pressure, obtained using 20 fs X-ray pulses at 17.8 keV and 2.2 MHz repetition, is illustrated through splitting of diffraction peaks, and interpreted employing finite element modeling of the sample chamber in the DAC.

Original language	English
Pages (from-to)	688-706
Number of pages	19
Journal	Journal of Synchrotron Radiation
Volume	28
DOIs	https://doi.org/10.1107/S1600577521002551
State	Published - May 1 2021

Keywords

Diamond anvil cells
Finite element modeling
High-precision X-ray diffraction
X-ray free-electron lasers

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10.1107/S1600577521002551

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Liermann, H. P., Konopkova, Z., Appel, K., Prescher, C., Schropp, A., Cerantola, V., Husband, R. J., McHardy, J. D., McMahon, M. I., McWilliams, R. S., Pepin, C. M., Mainberger, J., Roeper, M., Berghauser, A., Damker, H., Talkovski, P., Foese, M., Kujala, N., Ball, O. B., ... Strohm, C. (2021). Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL). Journal of Synchrotron Radiation, 28, 688-706. https://doi.org/10.1107/S1600577521002551

@article{1b62bdcfd41042388cd6ea7f911d7786,

title = "Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)",

abstract = "The high-precision X-ray diffraction setup for work with diamond anvil cells (DACs) in interaction chamber 2 (IC2) of the High Energy Density instrument of the European X-ray Free-Electron Laser is described. This includes beamline optics, sample positioning and detector systems located in the multipurpose vacuum chamber. Concepts for pump-probe X-ray diffraction experiments in the DAC are described and their implementation demonstrated during the First User Community Assisted Commissioning experiment. X-ray heating and diffraction of Bi under pressure, obtained using 20 fs X-ray pulses at 17.8 keV and 2.2 MHz repetition, is illustrated through splitting of diffraction peaks, and interpreted employing finite element modeling of the sample chamber in the DAC.",

keywords = "Diamond anvil cells, Finite element modeling, High-precision X-ray diffraction, X-ray free-electron lasers",

author = "Liermann, \{H. P.\} and Z. Konopkova and K. Appel and C. Prescher and A. Schropp and V. Cerantola and Husband, \{R. J.\} and McHardy, \{J. D.\} and McMahon, \{M. I.\} and McWilliams, \{R. S.\} and Pepin, \{C. M.\} and J. Mainberger and M. Roeper and A. Berghauser and H. Damker and P. Talkovski and M. Foese and N. Kujala and Ball, \{O. B.\} and Baron, \{M. A.\} and R. Briggs and M. Bykov and E. Bykova and J. Chantel and Coleman, \{A. L.\} and H. Cynn and D. Dattelbaum and Dresselhaus-Marais, \{L. E.\} and Eggert, \{J. H.\} and L. Ehm and Evans, \{W. J.\} and G. Fiquet and M. Frost and K. Glazyrin and Goncharov, \{A. F.\} and H. Hwang and Zs Jenei and Kim, \{J. Y.\} and F. Langenhorst and Y. Lee and M. Makita and H. Marquardt and McBride, \{E. E.\} and S. Merkel and G. Morard and O'Bannon, \{E. F.\} and C. Otzen and Pace, \{E. J.\} and A. Pelka and Pigott, \{J. S.\} and Prakapenka, \{V. B.\} and R. Redmer and C. Sanchez-Valle and M. Schoelmerich and S. Speziale and G. Spiekermann and Sturtevant, \{B. T.\} and S. Toleikis and N. Velisavljevic and M. Wilke and Yoo, \{C. S.\} and C. Baehtz and U. Zastrau and C. Strohm",

year = "2021",

month = may,

day = "1",

doi = "10.1107/S1600577521002551",

language = "English",

volume = "28",

pages = "688--706",

journal = "Journal of Synchrotron Radiation",

issn = "0909-0495",

}

Liermann, HP, Konopkova, Z, Appel, K, Prescher, C, Schropp, A, Cerantola, V, Husband, RJ, McHardy, JD, McMahon, MI, McWilliams, RS, Pepin, CM, Mainberger, J, Roeper, M, Berghauser, A, Damker, H, Talkovski, P, Foese, M, Kujala, N, Ball, OB, Baron, MA, Briggs, R, Bykov, M, Bykova, E, Chantel, J, Coleman, AL, Cynn, H, Dattelbaum, D, Dresselhaus-Marais, LE, Eggert, JH, Ehm, L, Evans, WJ, Fiquet, G, Frost, M, Glazyrin, K, Goncharov, AF, Hwang, H, Jenei, Z, Kim, JY, Langenhorst, F, Lee, Y, Makita, M, Marquardt, H, McBride, EE, Merkel, S, Morard, G, O'Bannon, EF, Otzen, C, Pace, EJ, Pelka, A, Pigott, JS, Prakapenka, VB, Redmer, R, Sanchez-Valle, C, Schoelmerich, M, Speziale, S, Spiekermann, G, Sturtevant, BT, Toleikis, S, Velisavljevic, N, Wilke, M, Yoo, CS, Baehtz, C, Zastrau, U & Strohm, C 2021, 'Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)', Journal of Synchrotron Radiation, vol. 28, pp. 688-706. https://doi.org/10.1107/S1600577521002551

TY - JOUR

T1 - Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)

AU - Liermann, H. P.

AU - Konopkova, Z.

AU - Appel, K.

AU - Prescher, C.

AU - Schropp, A.

AU - Cerantola, V.

AU - Husband, R. J.

AU - McHardy, J. D.

AU - McMahon, M. I.

AU - McWilliams, R. S.

AU - Pepin, C. M.

AU - Mainberger, J.

AU - Roeper, M.

AU - Berghauser, A.

AU - Damker, H.

AU - Talkovski, P.

AU - Foese, M.

AU - Kujala, N.

AU - Ball, O. B.

AU - Baron, M. A.

AU - Briggs, R.

AU - Bykov, M.

AU - Bykova, E.

AU - Chantel, J.

AU - Coleman, A. L.

AU - Cynn, H.

AU - Dattelbaum, D.

AU - Dresselhaus-Marais, L. E.

AU - Eggert, J. H.

AU - Ehm, L.

AU - Evans, W. J.

AU - Fiquet, G.

AU - Frost, M.

AU - Glazyrin, K.

AU - Goncharov, A. F.

AU - Hwang, H.

AU - Jenei, Zs

AU - Kim, J. Y.

AU - Langenhorst, F.

AU - Lee, Y.

AU - Makita, M.

AU - Marquardt, H.

AU - McBride, E. E.

AU - Merkel, S.

AU - Morard, G.

AU - O'Bannon, E. F.

AU - Otzen, C.

AU - Pace, E. J.

AU - Pelka, A.

AU - Pigott, J. S.

AU - Prakapenka, V. B.

AU - Redmer, R.

AU - Sanchez-Valle, C.

AU - Schoelmerich, M.

AU - Speziale, S.

AU - Spiekermann, G.

AU - Sturtevant, B. T.

AU - Toleikis, S.

AU - Velisavljevic, N.

AU - Wilke, M.

AU - Yoo, C. S.

AU - Baehtz, C.

AU - Zastrau, U.

AU - Strohm, C.

PY - 2021/5/1

Y1 - 2021/5/1

N2 - The high-precision X-ray diffraction setup for work with diamond anvil cells (DACs) in interaction chamber 2 (IC2) of the High Energy Density instrument of the European X-ray Free-Electron Laser is described. This includes beamline optics, sample positioning and detector systems located in the multipurpose vacuum chamber. Concepts for pump-probe X-ray diffraction experiments in the DAC are described and their implementation demonstrated during the First User Community Assisted Commissioning experiment. X-ray heating and diffraction of Bi under pressure, obtained using 20 fs X-ray pulses at 17.8 keV and 2.2 MHz repetition, is illustrated through splitting of diffraction peaks, and interpreted employing finite element modeling of the sample chamber in the DAC.

AB - The high-precision X-ray diffraction setup for work with diamond anvil cells (DACs) in interaction chamber 2 (IC2) of the High Energy Density instrument of the European X-ray Free-Electron Laser is described. This includes beamline optics, sample positioning and detector systems located in the multipurpose vacuum chamber. Concepts for pump-probe X-ray diffraction experiments in the DAC are described and their implementation demonstrated during the First User Community Assisted Commissioning experiment. X-ray heating and diffraction of Bi under pressure, obtained using 20 fs X-ray pulses at 17.8 keV and 2.2 MHz repetition, is illustrated through splitting of diffraction peaks, and interpreted employing finite element modeling of the sample chamber in the DAC.

KW - Diamond anvil cells

KW - Finite element modeling

KW - High-precision X-ray diffraction

KW - X-ray free-electron lasers

UR - https://www.scopus.com/pages/publications/85105502211

U2 - 10.1107/S1600577521002551

DO - 10.1107/S1600577521002551

M3 - Article

C2 - 33949979

AN - SCOPUS:85105502211

SN - 0909-0495

VL - 28

SP - 688

EP - 706

JO - Journal of Synchrotron Radiation

JF - Journal of Synchrotron Radiation

ER -

Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)

Abstract

Keywords

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