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Structure characterization of nanocomposites by synchrotron X-ray rays

  • Stony Brook University

Research output: Chapter in Book/Report/Conference proceedingConference contributionpeer-review

Abstract

The two most routinely used characterization techniques for determination of nanofiller morphology (e.g. exfoliation and intercalation of nanoclays, orientation of nanotubes) in polymer nanocomposites are transmission electron microscopy (TEM) and small-angle X-ray scattering (SAXS). The latter can be further used for in-situ and time-resolved studies. In this paper, we demonstrate that the use of three-dimension (3D) TEM and novel SAXS analysis can provide quantitative and complimentary structural information about clay orientation in polymer nanocomposites. In another part of the study, crystallization of model polyethylene blends (UHMWPE and low molecular weight polyethylene (MB-50k)) containing multi-walled carbon nanotubes (MWNT) was investigated by using in-situ rheo-X-ray techniques combining rheological and structural properties. The role of MWNT on the crystallization of model polyethylene blends at different temperature is discussed.

Original languageEnglish
Title of host publication2007 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2007, Technical Proceedings
Pages654-657
Number of pages4
StatePublished - 2007
Event2007 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2007 - Santa Clara, CA, United States
Duration: May 20 2007May 24 2007

Publication series

Name2007 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2007, Technical Proceedings
Volume1

Conference

Conference2007 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2007
Country/TerritoryUnited States
CitySanta Clara, CA
Period05/20/0705/24/07

Keywords

  • Carbon nanotubes
  • Organoclay
  • Polymer nanocomposite
  • SAXS
  • TEM

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